Applied Method Development for Gas Chromatography and Gas Chromatography - Mass Spectrometry
Description:
This course has been approved by the Royal Society of Chemistry for purposes of Continuing Professional Development.
The course examines the method development process for GC & GC-MS analysis in detail, covering the objectives of the analytical method and how to plan the method development process. The course looks in detail at the parameters that can be optimised and the order in which to optimise them in.
Participants will then implement the knowledge gained through practical method development case studies.
The course provides an introduction to method performance and looks at system validation protocols and how to validate the method, along with an introduction to analytical method accreditation.
The course has a strong focus on the practical information regarding the techniques, this knowledge can be utilised the instant you return to your lab.
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Instructor: Diane Turner - Anthias Consulting Ltd
Biography: Diane Turner is Founder, Director & Senior Consultant of Anthias Consulting Ltd. A Warwick University Graduate, Diane completed her Masters in analytical chemistry and started her career in environmental chemistry, later gaining significant experience as an Applications Chemist. Diane has developed methods for, given support and training for companies in most industries around the world for over 20 years. Diane is a visiting Academic & Consultant at The Open University where she continues her disease diagnosis research from her PhD. In 2019, Diane was elected as President of the Royal Society of Chemistry Analytical Division Council, serving from 2020 – 2022 and as Chair of the Analytical Chemistry Trust Fund. Diane is a Trustee of the Recycling Organisation for Research Opportunities. She is a member of the Government Chemist Programme Expert Group. Diane is co-author of 'Gas Chromatography-Mass Spectrometry: How Do I Get the Best Results?' published by the Royal Society of Chemistry.
Course Outline:
The course provides strategies for method development from research and planning, to the steps and parameters to consider at each stage of analysis, and how to optimise the parameters for each step. The course will cover:
Objectives of the method & research and planning
Autosamplers & automated sample preparation - how do I get my sample into GC?
Carrier gases and flow - how do I transport my sample into GC?
Sample introduction - how do I transfer my sample into column?
Separation & stationary phases - how do I choose my column?
Detection - how do I detect my analytes?
Sampling processes (blanks, spikes)
Getting stuck - strategies
Introduction to method performance
Instrument qualification & system validation
Introduction to accreditation
Learning Objectives:
You will learn strategies for method development.
You will learn how to optimise for sensitivity or to reduce carryover.
You will learn how to break the method down into tasks.
You will learn about the parameters and how to optimise them for each method task.
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Applied Method Development for Gas Chromatography and Gas Chromatography - Mass Spectrometry
Diane Turner - Anthias Consulting Ltd
Applied Method Development for Gas Chromatography and Gas Chromatography - Mass Spectrometry
Description
Session Number: SC248
Session Type: Short Courses
Session Date: Saturday 3/18/2023
Session Time: 8:30 AM - 5:00 PM
Room Number: Short Course Office 108B
Track: Professional Skills Building
Category: Gas Chromatography, Gas Chromatography/Mass Spectrometry, Separation Sciences
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