Solid Phase Microextraction: Theory and Practice
Description:
In this course several microextraction technologies will be discussed, namely solid phase microextraction (SPME), thin film microextraction (TFME) and needle trap devices (NT). The main
principles of these techniques, different calibration methods, coupling strategies to GC, LC, and MS, method development steps, and advantages and disadvantages of each microextraction approach will be covered. In addition, during this short course, recent advances, developments and applications of each technique in fields such as forensic, environmental, food and flavor, and clinical analysis will be described. Other topics that will be covered involve the application of SPME for ligand-receptor binding and plasma protein binding studies, in vivo sampling of freely moving animals for pharmacokinetic and metabolomic studies, direct tissue analysis, and automation of SPME and related technologies in high-throughput format.
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Instructor: Khaled Murtada - University of Waterloo
Biography: Dr. Khaled Murtada is a postdoctoral scientist with the Department of Chemistry at the University of Waterloo (ON, Canada) working with Professor Janusz Pawliszyn, who is also co-instructor in the course. Dr. Murtada's research focuses on the development of green analytical methods for environmental, food, and bio-analysis applications using CE, GC-MS, and LC-MS/MS. Additionally, Dr. Murtada is interested in the synthesis and characterization of new nanomaterials for use as tools in analytical chemistry.
Course Outline:
Introduction to solventless technologies, Theoretical principles of SPME, TFME and NT, Interfaces, Calibration, Method development, Automation, In-vivo sampling, Drug and clinical analysis, Food,
flavor and fragrance analysis, Environmental analysis, and Direct coupling of different SPME formats with mass spectrometry.
Learning Objectives:
Solventless technologies, Theoretical principles of SPME, TFME and NT, Interfaces, Calibration, Method development, Automation, In-vivo sampling, Drug and clinical analysis, Food, flavor and fragrance analysis, Environmental analysis, and Direct coupling of different SPME formats with mass spectrometry.
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Solid Phase Microextraction: Theory and Practice
Khaled Murtada - University of Waterloo
Solid Phase Microextraction: Theory and Practice
Description
Session Number: SC135
Session Type: Short Courses
Session Date: Sunday 3/19/2023
Session Time: 8:30 AM - 5:00 PM
Room Number: Short Course Office 108B
Track: Environmental
Category: Environmental, Gas Chromatography/Mass Spectrometry, Liquid Chromatography/Mass Spectrometry
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